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ABOUT SSL CERTIFICATES
Products»Hart Scientific»Primary Standards»Apparatus
 
Freeze-Point Furnaces (Models 9114, 9115, 9116)
Manufacturer: Hart Scientific
 

Features

  • Designed for long plateaus
  • Automated controllers, RS-232 included
  • Top access to high-stability Hart controllers
  • External cooling coils

Specifications

9114  9115A  9116 

Temperature Range 

100 °C to 680 °C 

550 °C to 1000 °C 

400 °C to 1100 °C 

Temperature Stability 

±0.03 °C 

±0.25 °C 

±0.5 °C 

Temperature Uniformity 

±0.05 °C
(±0.1 °C in the pre-heat well) 

+0.1 °C 

less than +0.5 °C 

Set-Point Accuracy 

±0.5 °C 

±3.0 °C 

Set-Point Resolution 

0.01 °C 

0.1 °C 

Display Resolution 

0.01 °C 

0.1 °C below 1000 °C
1 °C above 1000 °C 

Thermal Safety Cutout Accuracy 

±5 °C 

±10 °C 

Heater Power 

End Zones:
1000 W each
(at 230 VAC nominal)
Primary Zone:
1500 W 

2500 W 

End Zones:
800 W each
(at 230 VAC nominal)
Primary Zone: 900 W 

Exterior Dimensions (HxWxD) 

838 x 610 x 406 mm
(33 x 24 x 16 in) 

Power Requirements 

230 VAC (±10 %), 50/60 Hz, 1 Phase, 12 A maximum 

Weight 

92 kg (203 lb.) 

82 kg (180 lb.) 

68 kg (150 lb.) 

This furnace has a range of 100 °C to 680 °C, which includes the indium, tin, zinc, and aluminum fixed points, all in one furnace. 

The 9114 furnace has an inlet for use of clean dry air or inert gas to initiate the supercool of a tin cell. Other furnaces require the user to remove the hot and fragile tin cell from the furnace by hand before cooling. In a Hart furnace, you simply turn on your gas, monitor your cell during its supercool, and turn the gas off when the freeze begins. 

The 9114 is a three-zone furnace with the best in Hart digital controller technology. Hart designs and builds proprietary controllers that have a reputation of being the best in the business. All of our fixed-point furnaces use them to achieve excellent stability and uniformity. 

For easy access and visibility, all three zones are controlled from the top of the unit. The primary controller can be set in 0.01 °C increments, and actual temperature is readable to two decimal places. 

The freezing and melting process can be automated using eight preset, user-
programmable temperature settings. The top and bottom zones are slaved to the primary zone using differential thermocouples. A high-temperature PRT acts as the main control sensor for the best accuracy, sensitivity, and repeatability. 

 9115A

The 9115A Sodium Heat Pipe Furnace is specifically designed for maintenance of aluminum and silver freeze-point cells. 

It has a temperature range of 550 °C
to 1000 °C with gradients of less than ±0.1 °C throughout. The sodium heat-pipe design provides a simple, yet uniform, single heating zone that ensures very uniform changes in states during heating and cooling. 

Melting, freeze initiation, and plateau control for a variety of freeze-point cells are possible by entering up to eight set-points, ramp rates, and soak times. The controller displays temperature in degrees C or F, and temperature feedback is done via a thermocouple. Freeze-point plateaus of 8 to 10 hours are typical, and 24 hours are possible under controlled conditions. 

External cooling coils are included for circulation of tap water to reduce chassis temperature and heat load to the lab. Temperature cutouts protect your SPRTs and the furnace from exposure to excessive temperatures. 

 9116

Designed to be used with thermocouples and HTSPRTs the 9116 can reach temperatures up to 1100°C. Primarily designed for use at the copper point, the 9116 may also be optimized at the factory for silver and aluminum fixed points.  However to calibrate probes less than ~25 inches in length a 9114 must be used instead. 

The freezing and melting process may be automated using eight preset, user-programmable temperature settings. The top and bottom zones are slaved to the primary zone using differential thermocouples. A thermocouple acts as the main control sensor for the best accuracy, sensitivity, and repeatability. 

The 9116 has all of the standard features found on other Hart freeze-point furnaces, including external cooling coils and an RS-232 port

 

2127

Specifications - 2127 

Dimensions 

2127-9114: 54 mm x 510 mm
2127-9115: 62 mm x 510 mm
2127-9116: 54 mm x 510 mm 

Wells 

Three: 8 mm ID x 488 mm 
(0.31 x 19.2 in) 

Immersion Protection 

Last 156 mm (6.1 in) in alumina 

Well-to-Well Uniformity 

10 mK at 660 °C in 9114 

Temperature Range 

Up to 1100 °C 

Freeze-Point Furnaces
 
 Resources
PDF File – Requires Adobe Reader Data Sheet
PDF File – Requires Adobe Reader 9114 User Guide
PDF File – Requires Adobe Reader 9115 User Guide
PDF File – Requires Adobe Reader 9116 User Guide
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